宇航计测技术

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原子层沉积纳米钝化层薄膜厚度测量技术研究

李建国1;惠龙飞1;秦利军1;龚婷1;张王乐1   

  1. 1、西安近代化学研究所,陕西西安 710065
  • 出版日期:2019-06-25 发布日期:2019-06-25
  • 作者简介:李建国(1986.08-),助理研究员,硕士,主要研究方向:原子层沉积设备开发、原子层沉积在粉体材料表面修饰及功能薄膜制备等技术。

Research on In-situ Thickness Measurement of Atomic Layer #br# Deposition Nano-Passivation Layers

LI Jian-guo1;HUI Long-fei1;QIN Li-jun;1GONG Ting1;ZHANG Wang-le1   

  1. 1、Xian Modern Chemistry Research Institute,Xian 710065,China
  • Online:2019-06-25 Published:2019-06-25

摘要: 原子层沉积无机纳米薄膜技术广泛应用于军民领域。本文通过在原子层沉积系统加装原位石英晶体微天平测量系统,通过原位石英晶体微天平研究原子层沉积无机薄膜生长过程并进行薄膜厚度的在线测量。通过研究原子层沉积反应条件,实现原子层沉积无机薄膜厚度的石英晶体微天平在线测量结果替代薄膜厚度线下光学测量结果,解决各类复杂腔体内壁原子层沉积薄膜厚度无法精确测量的问题。

关键词: 原子层沉积, 石英晶体微天平, 原位测量

Abstract: Atomic layer deposition of inorganic nano-film technology is widely used in military and civilian applications.In this paper,the in-situ quartz crystal microbalance measurement system was used to study the growth process of atomic layer deposition inorganic film,and the film thickness was measured by quartz crystal microbalance.By studying the atomic layer deposition reaction conditions,the in-situ measurement results of the inorganic film thickness of the atomic layer deposition are used instead of the optical measurement results of the film thickness.It can solve the problem that the thickness of the atomic layer deposited film in various complex chambers cannot be accurately measured.

Key words: Atomic layer deposition, Quartz crystal microbalance, In-situ measurement